Microscale and Macroscale Techniques in the Organic Laboratory

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9780030343117: Microscale and Macroscale Techniques in the Organic Laboratory
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The well-known and tested organic chemistry laboratory techniques of the two best-selling organic chemistry lab manuals: INTRODUCTION TO ORGANIC LABORATORY TECHNIQUES: A SMALL SCALE APPROACH and INTRODUCTION TO ORGANIC LABORATORY TECHNIQUES: A MICROSCALE APPROACH, 3/e are now assembled in one textbook. Professors can use any experiments alongside MICROSCALE AND MACROSCALE TECHNIQUES IN THE ORGANIC LABORATORY. Experiments can be selected and assembled from the two Pavia organic chemistry lab manuals, from professors' homegrown labs, or even competing texts. The 375 page, hardcover book serves as a reference for all students of organic chemistry. With clearly written prose and accurately drawn diagrams, students can feel confident setting up and running organic labs.

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Donald L. Pavia earned his BS degree in chemistry from Reed College and his PhD in organic chemistry from Yale University. In 1970, he joined the faculty at Western Washington University as Assistant Professor and now holds the rank of Professor Emeritus. He is the coauthor of two organic laboratory books that include techniques and experiments: INTRODUCTION TO ORGANIC LABORATORY TECHNIQUES: A MICROSCALE APPROACH (Cengage Learning), and A SMALL SCALE APPROACH TO ORGANIC LABORATORY TECHNIQUES (Cengage Learning), as well as MICROSCALE AND MACROSCALE TECHNIQUES IN THE ORGANIC LABORATORY (Cengage Learning), which highlights techniques to be used with a faculty member's own experiments. He is a co-author, with Gary M. Lampman, George S. Kriz and James R. Vyvyan of an organic spectroscopy book, INTRODUCTION TO SPECTROSCOPY (Cengage Learning). Professor Pavia's research interests center on the synthesis and reactions of valence tautomeric and photochromic compounds, especially pyrylium-3-oxide tautomers. Autoxidations are a special interest. His other interests include the use of computers in teaching organic chemistry, both for lecture presentation and for the simulation of laboratories. He is the author of several computer programs. One such program is SQUALOR (Simulated Qualitative Organic Analysis) for which he won the 1986 EDUCOM/NCRIPTAL award. The program is designed for teaching the methods for solving organic unknowns.

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1. Laboratory Safety. 2. Advance Preparation and Laboratory Records. 3. Laboratory Glassware. 4. How to Find Data for Your Compound: Handbooks and Catalogues. 5. Measurement of Volume and Weight. 6. Heating and Cooling Methods. 7. Reaction Methods. 8. Filtration. 9. Physical Constants of Solids: The Melting Point. 10. Solubility. 11. Crystallization: Purification of Solids. 12. Extractions, Separations, and Drying Agents. 13. Physical Constants of Liquids: Boiling Point and Density. 14. Simple Distillation. 15. Fractional Distillation; Azeotropes. 16. Vacuum Distillation; Manometers. 17. Sublimation. 18. Steam Distillation. 19. Column Chromatography. 20. Thin-Layer Chromatography. 21. High-Performance Liquid Chromatography (HPLC). 22. Gas Chromatography. 23. Polarimetry. 24. Refractometry. 25. Infrared Spectroscopy. 26. Nuclear Magnetic Resonance Spectroscopy (Proton NMR). 27. Carbon-13 Nuclear Magnetic Resonance Spectroscopy. 28. Mass Spectrometry. 29. Computational Chemistry. 30. Guide to the Chemical Literature.

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9780495292470: Microscale and Macroscale Techniques in the Organic Laboratory

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