Laboratory Techniques for Organic Chemistry

4 avg rating
( 4 ratings by Goodreads )
 
9780871507037: Laboratory Techniques for Organic Chemistry

It includes a discussion of related theoretical material for each technique and safety notes throughout. Each chapter ends with a set of study problems that stress both the theoretical and practical aspects of each technique.

"synopsis" may belong to another edition of this title.

About the Author:

Ph.D., University of California, Berkeley

Review:

INTRODUCTION TO THE ORGANIC LABORATORY Safety in the Laboratory / The Laboratory Notebook / Laboratory Equipment 1. CRYSTALLIZATION Solvents for Crystallization / Steps in Crystallization / Supplemental Procedures 2. MELTING POINTS Characteristics of Melting Points / Melting-Point Apparatus / Steps in Determining a Melting Point / Supplemental Procedures 3. EXTRACTION Immiscible Liquids / Distribution Coefficients / Extraction Solvents / Chemically Active Extraction / Steps in Extractions / Additional Techniques Used in Extractions / Other Extraction Techniques 4. DRYING ORGANIC SOLUTIONS Extraction with Aqueous Sodium Chloride / Solid Inorganic Drying Agents / Procedure for Using Solid Inorganic Drying Agents / Azeotropic Drying 5. SIMPLE DISTILLATION Characteristics of Distillation / Steps in a Simple Distillation / Microscale and Semi-Microscale Distillation 6. FRACTIONAL DISTILLATION Efficiency of the Fractionation Column / Steps in Fractional Distillation / Microscale Fractional Distillation 7. VACUUM DISTILLATION Boiling Point and Pressure / Apparatus for Simple Vacuum Distillation / Steps in Vacuum Distillation 8. STEAM DISTILLATION Characteristics of Steam Distillation / Calculation of the Amount of Water Needed in a Steam Distillation / Apparatus for Steam Distillation 9. SUBLIMATION Atmospheric Sublimation / Vacuum Sublimation 10. REFRACTIVE INDEX Correcting for Temperature Differences / Steps in Using a Refractometer 11. COLUMN CHROMATOGRAPHY Gravity Column Chromatography. Flash Chromatography (Macroscale) / Flash Chromatography (Microscale) / High-Performance Liquid Chromatography (HPLC) 12. THIN LAYER CHROMATOGRAPHY The RF Value / Equipment for TLC / Steps in a TLC Analysis / A Related Technique: Paper Chromatography 13. GAS CHROMATOGRAPHY Gas Chromatography / The Gas Chromatograph / Steps in a GC Analysis / Problems Encountered in GC / Uses of Gas Chromatograms 14. CARRYING OUT TYPICAL REACTIONS Stirring / Heating Reaction Mixtures / Controlling Exothermic Reactions / Adding Reagents to a Reaction Mixture. Excluding Moisture from a Reaction Mixture / Setting Up a Three-Neck Reaction Flask / Hydrogen Halide Gas Traps 15. INFRARED SPECTROSCOPY The Infrared Spectrum / Absorption of Infrared Radiation / Interpreting Infrared Spectra / Identifying Types of Compounds / Preparing a Sample for an Infrared Spectrum / Instrumentation 16. PROTON NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY The NMR Spectrum / Interpreting NMR Spectra / Use of Deuterium in Proton NMR Spectroscopy / NMR Spectra of Unknowns / The NMR Spectrometer / Preparing Samples for NMR Spectra 17. THE CHEMICAL LITERATURE Introduction to the Chemical Literature / Secondary Literature / Primary Literature / APPENDIX I. COMMONLY USED CALCULATIONS / Molarity / Normality / Dilutions / Percent Concentrations / Percent Yields and Theoretical Yields / APPENDIX II / ELEMENTAL ANALYSES / Determining the Empirical Formula / Determining the Molecular Formula / Interpreting the Results of Elemental Analysis / Degree of Unsaturation / APPENDIX III. HEALTH HAZARDS OF COMPOUNDS USED IN ORGANIC CHEMISTRY / Where to Find Chemical Hazard Information / Understanding Health Hazard Warnings

"About this title" may belong to another edition of this title.

Top Search Results from the AbeBooks Marketplace

1.

Ralph J. Fessenden, Joan S. Fessenden
Published by Brooks/Cole
ISBN 10: 087150703X ISBN 13: 9780871507037
Used Paperback Quantity Available: 1
Seller:
OwlsBooks
(Toledo, OH, U.S.A.)
Rating
[?]

Book Description Brooks/Cole. Paperback. Book Condition: VERY GOOD. Light rubbing wear to cover, spine and page edges. Very minimal writing or notations in margins not affecting the text. Possible clean ex-library copy, with their stickers and or stamp(s). Bookseller Inventory # 2511959086

More Information About This Seller | Ask Bookseller a Question

Buy Used
US$ 3.65
Convert Currency

Add to Basket

Shipping: FREE
Within U.S.A.
Destination, Rates & Speeds

2.

Fessenden
Published by Brooks/Cole
ISBN 10: 087150703X ISBN 13: 9780871507037
Used Paperback Quantity Available: 1
Seller:
ThriftBooks - Green Earth
(Portland, OR, U.S.A.)
Rating
[?]

Book Description Brooks/Cole. Paperback. Book Condition: Fair. Bookseller Inventory # G087150703XI5N00

More Information About This Seller | Ask Bookseller a Question

Buy Used
US$ 3.89
Convert Currency

Add to Basket

Shipping: FREE
Within U.S.A.
Destination, Rates & Speeds

3.

Fessenden, Ralph J., Fessenden, Joan S.
Published by Brooks/Cole
ISBN 10: 087150703X ISBN 13: 9780871507037
Used Quantity Available: 1
Seller:
Wonder Book
(Frederick, MD, U.S.A.)
Rating
[?]

Book Description Brooks/Cole. Book Condition: Good. . Owner's name inside.Highlighting inside. Bookseller Inventory # S17C-00645

More Information About This Seller | Ask Bookseller a Question

Buy Used
US$ 4.09
Convert Currency

Add to Basket

Shipping: FREE
Within U.S.A.
Destination, Rates & Speeds

4.

Fessenden, Ralph J.; Fessenden, Joan S.
Published by Brooks/Cole (1984)
ISBN 10: 087150703X ISBN 13: 9780871507037
Used Paperback Quantity Available: 1
Seller:
Allied Book Company Inc.
(Ligonier, IN, U.S.A.)
Rating
[?]

Book Description Brooks/Cole, 1984. Paperback. Book Condition: Used: Acceptable. Book Leaves in 1 Business Day or Less! Leaves Same Day if Received by 2 pm EST! Cover is worn, mostly corners and binding. Acceptable. Bookseller Inventory # 106-04-00109

More Information About This Seller | Ask Bookseller a Question

Buy Used
US$ 3.77
Convert Currency

Add to Basket

Shipping: US$ 4.00
Within U.S.A.
Destination, Rates & Speeds

5.

Ralph J. Fessenden; Joan S. Fessenden
Published by Brooks/Cole (1984)
ISBN 10: 087150703X ISBN 13: 9780871507037
Used Paperback Quantity Available: 1
Seller:
Ergodebooks
(RICHMOND, TX, U.S.A.)
Rating
[?]

Book Description Brooks/Cole, 1984. Paperback. Book Condition: Used: Good. Bookseller Inventory # SONG087150703X

More Information About This Seller | Ask Bookseller a Question

Buy Used
US$ 7.23
Convert Currency

Add to Basket

Shipping: US$ 4.99
Within U.S.A.
Destination, Rates & Speeds