DEVELOPMENT OF ANALYTICAL TECHNIQUE FOR DETERMINATION OF METRONIDAZOLE: IN COMMERCIALLY AVAILABLE SUSPENSIONS

 
9783639277142: DEVELOPMENT OF ANALYTICAL TECHNIQUE FOR DETERMINATION OF METRONIDAZOLE: IN COMMERCIALLY AVAILABLE SUSPENSIONS

A simple and rapid HPLC assay procedure has been developed and validated for the quantitative determination of metronidazole benzoate from commercially available preparations. The HPLC system was developed based on the BP 2007 monograph of metronidazole suspension. However the various parameters were modified according to column and equipment available. The HPLC conditions used were, column: C18, detection: UV at 254 nm; injection volume: 20 ?l; mobile phase: methanol and de-ionized water (13:8, v/v); flow rate 1.0 ml min?1. The procedure separated metronidazole benzoate, in an overall analysis time of about 10 minutes with metronidazole benzoate eluting at about 7.7 minutes. The new method was evaluated by different validation parameters like specificity, sensitivity, accuracy and precision. The procedure provided a linear response over the concentration range 50?1000 ?gml?1.The metronidazole raw material as well as different commercially available suspensions containing metronidazole benzoate have been analysed by this method. The results obtained were accurate and precise showing no interference by the excipients in the products.

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About the Author:

Mr. Shafique Hussain passed his B.Pharmacy from Punjab University, Lahore in 2005. Then he passed his M.Phil in Pharmaceutical Chemistry from the same university in 2009. Now a days he is working as Hospital Pharmacist in Mayo Hospital Lahore Which is a teaching Hospital.

Mr. Shafique Hussain passed his B.Pharmacy from Punjab University, Lahore in 2005. Then he passed his M.Phil in Pharmaceutical Chemistry from the same university in 2009. Now a days he is working as Hospital Pharmacist in Mayo Hospital Lahore Which is a teaching Hospital.

Mr. Shafique Hussain passed his B.Pharmacy from Punjab University, Lahore in 2005. Then he passed his M.Phil in Pharmaceutical Chemistry from the same university in 2009. Now a days he is working as Hospital Pharmacist in Mayo Hospital Lahore Which is a teaching Hospital.

About the Author:

Mr. Shafique Hussain passed his B.Pharmacy from Punjab University, Lahore in 2005. Then he passed his M.Phil in Pharmaceutical Chemistry from the same university in 2009. Now a days he is working as Hospital Pharmacist in Mayo Hospital Lahore Which is a teaching Hospital.

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Hussain, Shafique; Saeed-ul-Hassan, Syed; Usman, M.
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Hussain, Shafique; Saeed-ul-Hassan, Syed; Usman, M.
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Book Description Book Condition: New. Publisher/Verlag: VDM Verlag Dr. Müller | IN COMMERCIALLY AVAILABLE SUSPENSIONS | A simple and rapid HPLC assay procedure has been developed and validated for the quantitative determination of metronidazole benzoate from commercially available preparations. The HPLC system was developed based on the BP 2007 monograph of metronidazole suspension. However the various parameters were modified according to column and equipment available. The HPLC conditions used were, column: C18, detection: UV at 254 nm; injection volume: 20 l; mobile phase: methanol and de-ionized water (13:8, v/v); flow rate 1.0 ml min 1. The procedure separated metronidazole benzoate, in an overall analysis time of about 10 minutes with metronidazole benzoate eluting at about 7.7 minutes. The new method was evaluated by different validation parameters like specificity, sensitivity, accuracy and precision. The procedure provided a linear response over the concentration range 50 1000 gml 1.The metronidazole raw material as well as different commercially available suspensions containing metronidazole benzoate have been analysed by this method. The results obtained were accurate and precise showing no interference by the excipients in the products. | Format: Paperback | Language/Sprache: english | 112 pp. Bookseller Inventory # K9783639277142

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Hussain, Shafique; Saeed-ul-Hassan, Syed; Usman, M.
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Hussain, Shafique; Saeed-ul-Hassan, Syed; Usman, M.
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Book Description VDM Verlag Nov 2010, 2010. Taschenbuch. Book Condition: Neu. 220x150x7 mm. Neuware - A simple and rapid HPLC assay procedure has been developed and validated for the quantitative determination of metronidazole benzoate from commercially available preparations. The HPLC system was developed based on the BP 2007 monograph of metronidazole suspension. However the various parameters were modified according to column and equipment available. The HPLC conditions used were, column: C18, detection: UV at 254 nm; injection volume: 20 l; mobile phase: methanol and de-ionized water (13:8, v/v); flow rate 1.0 ml min 1. The procedure separated metronidazole benzoate, in an overall analysis time of about 10 minutes with metronidazole benzoate eluting at about 7.7 minutes. The new method was evaluated by different validation parameters like specificity, sensitivity, accuracy and precision. The procedure provided a linear response over the concentration range 50 1000 gml 1.The metronidazole raw material as well as different commercially available suspensions containing metronidazole benzoate have been analysed by this method. The results obtained were accurate and precise showing no interference by the excipients in the products. 112 pp. Englisch. Bookseller Inventory # 9783639277142

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Hussain, Shafique; Saeed-ul-Hassan, Syed; Usman, M.
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Book Description VDM Verlag Nov 2010, 2010. Taschenbuch. Book Condition: Neu. 220x150x7 mm. Neuware - A simple and rapid HPLC assay procedure has been developed and validated for the quantitative determination of metronidazole benzoate from commercially available preparations. The HPLC system was developed based on the BP 2007 monograph of metronidazole suspension. However the various parameters were modified according to column and equipment available. The HPLC conditions used were, column: C18, detection: UV at 254 nm; injection volume: 20 l; mobile phase: methanol and de-ionized water (13:8, v/v); flow rate 1.0 ml min 1. The procedure separated metronidazole benzoate, in an overall analysis time of about 10 minutes with metronidazole benzoate eluting at about 7.7 minutes. The new method was evaluated by different validation parameters like specificity, sensitivity, accuracy and precision. The procedure provided a linear response over the concentration range 50 1000 gml 1.The metronidazole raw material as well as different commercially available suspensions containing metronidazole benzoate have been analysed by this method. The results obtained were accurate and precise showing no interference by the excipients in the products. 112 pp. Englisch. Bookseller Inventory # 9783639277142

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Hussain, Shafique; Saeed-ul-Hassan, Syed; Usman, M.
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Book Description VDM Verlag, Germany, 2010. Paperback. Book Condition: New. 220 x 150 mm. Language: English . Brand New Book. A simple and rapid HPLC assay procedure has been developed and validated for the quantitative determination of metronidazole benzoate from commercially available preparations. The HPLC system was developed based on the BP 2007 monograph of metronidazole suspension. However the various parameters were modified according to column and equipment available. The HPLC conditions used were, column: C18, detection: UV at 254 nm; injection volume: 20 l; mobile phase: methanol and de-ionized water (13:8, v/v); flow rate 1.0 ml min 1. The procedure separated metronidazole benzoate, in an overall analysis time of about 10 minutes with metronidazole benzoate eluting at about 7.7 minutes. The new method was evaluated by different validation parameters like specificity, sensitivity, accuracy and precision. The procedure provided a linear response over the concentration range 50-1000 gml 1.The metronidazole raw material as well as different commercially available suspensions containing metronidazole benzoate have been analysed by this method. The results obtained were accurate and precise showing no interference by the excipients in the products. Bookseller Inventory # KNV9783639277142

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Hussain, Shafique; Saeed-ul-Hassan, Syed; Usman, M.
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Hussain, Shafique; Saeed-ul-Hassan, Syed; Usman, M.
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Book Description VDM Verlag Nov 2010, 2010. Taschenbuch. Book Condition: Neu. 220x150x7 mm. This item is printed on demand - Print on Demand Neuware - A simple and rapid HPLC assay procedure has been developed and validated for the quantitative determination of metronidazole benzoate from commercially available preparations. The HPLC system was developed based on the BP 2007 monograph of metronidazole suspension. However the various parameters were modified according to column and equipment available. The HPLC conditions used were, column: C18, detection: UV at 254 nm; injection volume: 20 l; mobile phase: methanol and de-ionized water (13:8, v/v); flow rate 1.0 ml min 1. The procedure separated metronidazole benzoate, in an overall analysis time of about 10 minutes with metronidazole benzoate eluting at about 7.7 minutes. The new method was evaluated by different validation parameters like specificity, sensitivity, accuracy and precision. The procedure provided a linear response over the concentration range 50 1000 gml 1.The metronidazole raw material as well as different commercially available suspensions containing metronidazole benzoate have been analysed by this method. The results obtained were accurate and precise showing no interference by the excipients in the products. 112 pp. Englisch. Bookseller Inventory # 9783639277142

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