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Epoxidations and Hydroperoxidations of α,β-Unsaturated Ketones: An Approach through Asymmetric Organocatalysis (Springer Theses) - Softcover

 
9783642435331: Epoxidations and Hydroperoxidations of α,β-Unsaturated Ketones: An Approach through Asymmetric Organocatalysis (Springer Theses)
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In this book, Corinna Reisinger describes a new organocatalytic asymmetric epoxidation of cyclic and acyclic a,ß-unsaturated ketones, using primary amine salts as catalysts, and hydrogen peroxide as an inexpensive and environmentally benign oxidant.

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Corinna Reisinger has developed a new organocatalytic asymmetric epoxidation of cyclic and acyclic α,β-unsaturated ketones. In this thesis, Corinna documents her methodology, using primary amine salts as catalysts, and hydrogen peroxide as an inexpensive and environmentally benign oxidant. She describes the unprecedented and powerful catalytic asymmetric hydro­peroxi­dation of α,β-enones, a process which produces optically active five-membered cyclic peroxyhemiketals in a single operation. She also proves the versatility and synthetic value of the cyclic peroxyhemiketals by converting them into highly enantioenriched acyclic and cyclic aldol products. Currently, these cyclic aldol products are inaccessible by any other synthetic means. Furthermore, cyclic peroxyhemiketals are precursors to optically active 1,2-dioxolanes which are of biological relevance. This work is a breakthrough in the field of asymmetric epoxidation chemistry and outlines the most efficient method in the literature for generating highly enantioselective cyclic epoxyketones known to date.

About the Author:
Dr. Corinna Reisinger Evonik AG corinna.reisinger@web.de

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  • PublisherSpringer
  • Publication date2014
  • ISBN 10 3642435335
  • ISBN 13 9783642435331
  • BindingPaperback
  • Number of pages276

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Book Description Taschenbuch. Condition: Neu. This item is printed on demand - it takes 3-4 days longer - Neuware -Corinna Reisinger has developed a new organocatalytic asymmetric epoxidation of cyclic and acyclic ,beta-unsaturated ketones. In this thesis, Corinna documents her methodology, using primary amine salts as catalysts, and hydrogen peroxide as an inexpensive and environmentally benign oxidant. She describes the unprecedented and powerful catalytic asymmetric hydroperoxidation of ,beta-enones, a process which produces optically active five-membered cyclic peroxyhemiketals in a single operation. She also proves the versatility and synthetic value of the cyclic peroxyhemiketals by converting them into highly enantioenriched acyclic and cyclic aldol products. Currently, these cyclic aldol products are inaccessible by any other synthetic means. Furthermore, cyclic peroxyhemiketals are precursors to optically active 1,2-dioxolanes which are of biological relevance. This work is a breakthrough in the field of asymmetric epoxidation chemistry and outlines the most efficient method in the literature for generating highly enantioselective cyclic epoxyketones known to date. 276 pp. Englisch. Seller Inventory # 9783642435331

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Book Description Condition: New. Dieser Artikel ist ein Print on Demand Artikel und wird nach Ihrer Bestellung fuer Sie gedruckt. Nominated by the Max-Planck-Institut fuer Kohlenforschung for a Springer Theses PrizeA breakthrough in the field of asymmetric epoxidation chemistryThis work could lead to numerous commercial applicationsCorinna Reisinger has deve. Seller Inventory # 5060821

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Book Description Taschenbuch. Condition: Neu. Druck auf Anfrage Neuware - Printed after ordering - Corinna Reisinger has developed a new organocatalytic asymmetric epoxidation of cyclic and acyclic ,beta-unsaturated ketones. In this thesis, Corinna documents her methodology, using primary amine salts as catalysts, and hydrogen peroxide as an inexpensive and environmentally benign oxidant. She describes the unprecedented and powerful catalytic asymmetric hydroperoxidation of ,beta-enones, a process which produces optically active five-membered cyclic peroxyhemiketals in a single operation. She also proves the versatility and synthetic value of the cyclic peroxyhemiketals by converting them into highly enantioenriched acyclic and cyclic aldol products. Currently, these cyclic aldol products are inaccessible by any other synthetic means. Furthermore, cyclic peroxyhemiketals are precursors to optically active 1,2-dioxolanes which are of biological relevance. This work is a breakthrough in the field of asymmetric epoxidation chemistry and outlines the most efficient method in the literature for generating highly enantioselective cyclic epoxyketones known to date. Seller Inventory # 9783642435331

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