RP-HPLC method for the determination of Anti-Anginal Drugs

 
9783659359651: RP-HPLC method for the determination of Anti-Anginal Drugs
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A simple, specific, accurate and precise stability indicating reverse phase high performance liquid chromatographic (RP-HPLC) method has been developed for the simultaneous estimation of Aspirin and Isosorbide 5-mononitrate in bulk drug and its pharmaceutical dosage form. A chromatographic separation was achieved with reverse phase phenomenex® Luna 5µ C18 (2) 100A (250 × 4.60 mm) column in an isocratic mode at ambient temperature. The mobile phase consisting of water: methanol: acetonitrile (55:28:17% v/v/v) at a flow rate of 1 ml/min. The eluents were monitored at 217 nm. The retention times of Aspirin and Isosorbide 5-mononitrate were found to be 2.05±0.056 min and 4.27±0.016 min respectively. The regression analysis revealed linearity in the concentration range of 1-10 µg/ml and 1-10 µg/ml for Aspirin and Isosorbide 5-mononitrate respectively. The method was validated in terms of linearity, accuracy, precision, limit of detection (LOD), limit of quantification (LOQ) in accordance with ICH guide lines. The results of the study showed that the developed method is simple, precise and accurate, and therefore suitable for routine analysis of these drugs in pharmaceutical dosage form.

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S.Hasan Amrohi obtained his Masters in Pharmaceutical Analysis & Quality Assurance in Lalitha college of Pharmacy. He is currently working as a Assistant Professor at School of Pharmacy, Anurag Group Of Institution. Research interests are primarily in the areas of RP-HPLC, GC, LC-MS/MS, Drug Discovery, Stability Studies and Impurity Profiling.

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Book Description Condition: New. Publisher/Verlag: LAP Lambert Academic Publishing | A simple, specific, accurate and precise stability indicating reverse phase high performance liquid chromatographic (RP-HPLC) method has been developed for the simultaneous estimation of Aspirin and Isosorbide 5-mononitrate in bulk drug and its pharmaceutical dosage form. A chromatographic separation was achieved with reverse phase phenomenex® Luna 5µ C18 (2) 100A (250 × 4.60 mm) column in an isocratic mode at ambient temperature. The mobile phase consisting of water: methanol: acetonitrile (55:28:17% v/v/v) at a flow rate of 1 ml/min. The eluents were monitored at 217 nm. The retention times of Aspirin and Isosorbide 5-mononitrate were found to be 2.05±0.056 min and 4.27±0.016 min respectively. The regression analysis revealed linearity in the concentration range of 1-10 µg/ml and 1-10 µg/ml for Aspirin and Isosorbide 5-mononitrate respectively. The method was validated in terms of linearity, accuracy, precision, limit of detection (LOD), limit of quantification (LOQ) in accordance with ICH guide lines. The results of the study showed that the developed method is simple, precise and accurate, and therefore suitable for routine analysis of these drugs in pharmaceutical dosage form. | Format: Paperback | Language/Sprache: english | 112 pp. Seller Inventory # K9783659359651

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Book Description LAP Lambert Academic Publishing Mrz 2013, 2013. Taschenbuch. Condition: Neu. Neuware - A simple, specific, accurate and precise stability indicating reverse phase high performance liquid chromatographic (RP-HPLC) method has been developed for the simultaneous estimation of Aspirin and Isosorbide 5-mononitrate in bulk drug and its pharmaceutical dosage form. A chromatographic separation was achieved with reverse phase phenomenex® Luna 5µ C18 (2) 100A (250 × 4.60 mm) column in an isocratic mode at ambient temperature. The mobile phase consisting of water: methanol: acetonitrile (55:28:17% v/v/v) at a flow rate of 1 ml/min. The eluents were monitored at 217 nm. The retention times of Aspirin and Isosorbide 5-mononitrate were found to be 2.05±0.056 min and 4.27±0.016 min respectively. The regression analysis revealed linearity in the concentration range of 1-10 µg/ml and 1-10 µg/ml for Aspirin and Isosorbide 5-mononitrate respectively. The method was validated in terms of linearity, accuracy, precision, limit of detection (LOD), limit of quantification (LOQ) in accordance with ICH guide lines. The results of the study showed that the developed method is simple, precise and accurate, and therefore suitable for routine analysis of these drugs in pharmaceutical dosage form. 112 pp. Englisch. Seller Inventory # 9783659359651

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Book Description LAP Lambert Academic Publishing Mrz 2013, 2013. Taschenbuch. Condition: Neu. Neuware - A simple, specific, accurate and precise stability indicating reverse phase high performance liquid chromatographic (RP-HPLC) method has been developed for the simultaneous estimation of Aspirin and Isosorbide 5-mononitrate in bulk drug and its pharmaceutical dosage form. A chromatographic separation was achieved with reverse phase phenomenex® Luna 5µ C18 (2) 100A (250 × 4.60 mm) column in an isocratic mode at ambient temperature. The mobile phase consisting of water: methanol: acetonitrile (55:28:17% v/v/v) at a flow rate of 1 ml/min. The eluents were monitored at 217 nm. The retention times of Aspirin and Isosorbide 5-mononitrate were found to be 2.05±0.056 min and 4.27±0.016 min respectively. The regression analysis revealed linearity in the concentration range of 1-10 µg/ml and 1-10 µg/ml for Aspirin and Isosorbide 5-mononitrate respectively. The method was validated in terms of linearity, accuracy, precision, limit of detection (LOD), limit of quantification (LOQ) in accordance with ICH guide lines. The results of the study showed that the developed method is simple, precise and accurate, and therefore suitable for routine analysis of these drugs in pharmaceutical dosage form. 112 pp. Englisch. Seller Inventory # 9783659359651

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Book Description LAP LAMBERT Academic Publishing. Paperback. Condition: New. 112 pages. Dimensions: 8.7in. x 5.9in. x 0.3in.A simple, specific, accurate and precise stability indicating reverse phase high performance liquid chromatographic (RP-HPLC) method has been developed for the simultaneous estimation of Aspirin and Isosorbide 5-mononitrate in bulk drug and its pharmaceutical dosage form. A chromatographic separation was achieved with reverse phase phenomenex Luna 5 C18 (2) 100A (250 4. 60 mm) column in an isocratic mode at ambient temperature. The mobile phase consisting of water: methanol: acetonitrile (55: 28: 17 vvv) at a flow rate of 1 mlmin. The eluents were monitored at 217 nm. The retention times of Aspirin and Isosorbide 5-mononitrate were found to be 2. 050. 056 min and 4. 270. 016 min respectively. The regression analysis revealed linearity in the concentration range of 1-10 gml and 1-10 gml for Aspirin and Isosorbide 5-mononitrate respectively. The method was validated in terms of linearity, accuracy, precision, limit of detection (LOD), limit of quantification (LOQ) in accordance with ICH guide lines. The results of the study showed that the developed method is simple, precise and accurate, and therefore suitable for routine analysis of these drugs in pharmaceutical dosage form. This item ships from multiple locations. Your book may arrive from Roseburg,OR, La Vergne,TN. Paperback. Seller Inventory # 9783659359651

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Amrohi S Hasan, Nazneen Afra, Rasheed Anas
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Book Description LAP Lambert Academic Publishing, United States, 2013. Paperback. Condition: New. Language: English . Brand New Book. A simple, specific, accurate and precise stability indicating reverse phase high performance liquid chromatographic (RP-HPLC) method has been developed for the simultaneous estimation of Aspirin and Isosorbide 5-mononitrate in bulk drug and its pharmaceutical dosage form. A chromatographic separation was achieved with reverse phase phenomenex(r) Luna 5u C18 (2) 100A (250 x 4.60 mm) column in an isocratic mode at ambient temperature. The mobile phase consisting of water: methanol: acetonitrile (55:28:17 v/v/v) at a flow rate of 1 ml/min. The eluents were monitored at 217 nm. The retention times of Aspirin and Isosorbide 5-mononitrate were found to be 2.05 0.056 min and 4.27 0.016 min respectively. The regression analysis revealed linearity in the concentration range of 1-10 ug/ml and 1-10 ug/ml for Aspirin and Isosorbide 5-mononitrate respectively. The method was validated in terms of linearity, accuracy, precision, limit of detection (LOD), limit of quantification (LOQ) in accordance with ICH guide lines. The results of the study showed that the developed method is simple, precise and accurate, and therefore suitable for routine analysis of these drugs in pharmaceutical dosage for. Seller Inventory # KNV9783659359651

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