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The Synthesis Of Metal Complexes With Macrocyclic Glyoxime Ether

Emin Karapinar

ISBN 10: 3659427292 / ISBN 13: 9783659427299
Published by LAP LAMBERT Academic Publishing
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Paperback. 96 pages. Dimensions: 8.7in. x 5.9in. x 0.2in.In this work, by the reaction of four different chloroglyoximes with 4-Amminobenzo15-Crown-5 in absolute ethanol, eight of new macrocylic glyoxime ether compounds and their Ni(II), Co(II) and Cu(II) complexes have been synthesized. For this, firstly chlorophenylglyoxime, p-tolylchloroglyoxime, p-chlorophenyl chloroglyoxime and 4-biphenylchloroglyoxime were synthesized according to previously reported literatures. Then novel glyoxime derivatives with macrocyclic glyoxime ethers by the reactions between these compounds with 4-amminobenzo15-crown-5 were obtained. The complexes of these ligands with metal chlorid salts have been formed. Finally, the UV-VIS, IR, AAS and 1H NMR spectroscopic properties of these compounds were investigated and clarified by the help of the results of elemental analyses and the spectroscopic methods. The content of this book is based on an experimental study for my Ph. D thesis submitted to Selcuk University, Konya, Turkey in 2002. This item ships from multiple locations. Your book may arrive from Roseburg,OR, La Vergne,TN. Bookseller Inventory # 9783659427299

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Bibliographic Details

Title: The Synthesis Of Metal Complexes With ...

Publisher: LAP LAMBERT Academic Publishing

Binding: Paperback

Book Condition:New

Book Type: Paperback

About this title

Synopsis:

In this work, by the reaction of four different chloroglyoximes with 4’-Amminobenzo[15-Crown-5] in absolute ethanol, eight of new macrocylic glyoxime ether compounds and their Ni(II), Co(II) and Cu(II) complexes have been synthesized. For this, firstly chlorophenylglyoxime, p-tolylchloroglyoxime, p-chlorophenyl chloroglyoxime and 4’-biphenylchloroglyoxime were synthesized according to previously reported literatures. Then novel glyoxime derivatives with macrocyclic glyoxime ethers by the reactions between these compounds with 4’-amminobenzo[15-crown-5] were obtained. The complexes of these ligands with metal chlorid salts have been formed. Finally, the UV-VIS, IR, AAS and 1H NMR spectroscopic properties of these compounds were investigated and clarified by the help of the results of elemental analyses and the spectroscopic methods. The content of this book is based on an experimental study for my Ph.D thesis submitted to Selcuk University, Konya, Turkey in 2002.

About the Author:

Emin Karapinar was born in 1973 in Ankara. He graduated from Selcuk University with B.Sc. degree in Chemistry Department in 1994. He received his M.Sc. degree from Pamukkale University in 1996. He completed his Ph.D studies in 2002 at the Selcuk University.He has been working as a faculty member at Pamukkale University since 1994.

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