Otto has put together the most explicit syntheses on the bulk production of psychedelic amphetamines, precursors and reductions. MDA, MDMA (XTC), DOB, TMA, PMA, MDEA (Eve), DOM (STP) & other popular stimulants, eg. methylcathinone, phenetermine, aminorex, ephedrine. It is easy reading yet, explicit, hardcore, psychedelic amphetamine chemistry. eg. Methylcathinone and other psycho-stimulants from non-list chemicals. Production of precursors from fertilizer, spices, barks, seeds and oils. Expanded metal & electrolytic reductions. Bulk production of reduction & list chemicals from solvents & common chemicals at the local hardware store. Hundreds of reactions are described, current drug laws and list chemicals. 400+ references. UV Laminated, index
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AMPHETAMINE LABORATORIES
Laboratory Statistics
MDMA Production
The Chemist
METHAMPHETAMINE LABORATORIES
Methamphetamine Terms
Primary Methamphetamine Production Methods
Production With the United States
Production Outside the United States
Global and Domestic Entry/Exit Seizures
Crystal Methamphetamine -- Ice
Methamphetamine Production Methods
Hazardous Waste
Hazardous Waste Cleanup
CHEMICALS AND THE LAW
Principal Provisions of the Chemical
Diversion Control Laws and Regulations
Special Surveillance List
Special Surveillance List Chemicals
Controlled Substance Analogue Act
AMPHETAMINES, METHYLAMPHETAMINES, EPHEDRINES, AMINOREX, AMINO KETONES & SUBSTITUTED PHENYLISOPROPYLAMINES
3,4-Methylenedioxy-N-methylamphetamine
3,4-Methylenedioxy-N-alkylamphetamines
MDMA Story
MDMA Production
MDMA Precursor Chemicals
Substituted-3,4-methylenedioxyamphetamines
4-Substituted-2,5-dimethoxyamphetamines
4-Bromo-2,5-dimethoxyphenylalkylamines
4-Bromo-2,5-Dimethoxy-Substituted N-Alkylphenylalkylamines
PMA (para-Methoxyamphetamine)
PMA Production
Ephedrine Alkaloids
Cathine
AMINOKETONES
Phentermines
2-Amino-5-aryloxazolines
REDUCTIONS USING METALS
USING ALUMINUM:
Aluminum Amalgam from Aluminum Shavings; from Aluminum Foil; from Aluminum Powder
Reduction of P-2-P Using Amalgamated Al Turnings
Methamphetamine; P-2-P + Aluminum Foil
Reduction of P-2-P Using Aluminum Turnings (Amalgamated) with Amine
Reduction: Aluminum Amalgam & Nitromethane
USING ZINC:
Phenylethylamines from B-Nitrostyrene: Zinc and Mercuric Bichloride
Reduction of Phenylnitroalcohols with Zinc
Phenylpropanolamine Preparation
USING IRON: Reductions Using Iron Filings
Phenylnitroalcohols to Phenylaminoalcohols
Ephedrine from 1-Phenyl-1,2-propanedione
Ephedrine from 1-Phenylpropan-1-ol-2-one
Preparation of Mercury Bichloride
Methylamine Hydrochloride Preparation
Other Methods of Preparation
N-Methylation of Amphetamines
ELECTROLYTIC REDUCTIONS
Electrolytic Reduction Apparatus
Electrolytic Production
Preparation of Amphetamine from Phenyl-2-nitropropene
Preparation of Methoxy-amphetamine
Electrolytic Reduction Apparatus Components
Electrolytic Reduction Apparatus
The Electrolytic Reduction
Drying of the Phenylalkylamine HCl
Purification and Precipitation of the Substituted Phenylalkylamine Salt
Purification of the HCl Salt From the Catholyte Liquor
Amphetamine from Electrolytic Reduction of P-2-P/P-2-P Oxime
Electrolytic Reduction Apparatus
Electrolytic Preparation of Methamphetamine
from 1-Phenyl-1-chloro-2-methylaminopropane
Phenylnitroalkenes From Benzaldehydes and Nitroalkanes
Phenyl-2-nitropropenes from Propenylbenzenes
Phenyl-2-nitropropenes from Pseudonitrosites
Pseudonitrosites From Substituted Propenylbenzenes
Preparation of Phenylnitropropanols
Manufacture of Phenyl-2-nitropropanol
Manufacture of Sodium Nitrite
Preparation of Ether from Ethanol
PREPARATION OF KETONES
Phenyl-2-propanone From Phenylacetic Acid
Phenyl-2-propanone Using Pyridine
Dehydrocarboxylation of Carboxylic Acids to Form Phenyl-2-propanone
Gas Phase Production of Phenyl-2-propanone
from Phenyl Acetic Acid and Acetic Acid Preparation of P-2-P Using Magnesia
Preparation of Manganous Oxide Catalyst
Benzyl-Methyl-Ketone Preparation Using Manganese Dioxide
Preparation of Propiophenone from Benzoic Acid and Propionic Acid
Large Scale Production of Propiophenone
Phenyl Acetic Acid Preparation
Benzyl Cyanide
More Preparations of Phenyl Acetic Acid:
Method One: Benzylmagnesium Chloride and Dry Ice
Method Two: Modified Willgerodt Reaction
Method Three: Ethylbenzene and Sodium Chromate
Benzyl Chloride from Toluene
Benzyl Chloride from Benzyl Alcohol
Substituted Phenyl-2-Propanones From Substituted Phenyl-2-Nitropropenes
Phenyl-2-Propanone From Monochloroacetone
Preparation of Monochloroacetone
Chlorination of Acetone
Fractionation
Stabilization of Chloroacetone
Phenyl-2-propanones From Propenylbenzenes
Preparation of Propiophenone
Preparation of P-2-P from 2-Phenylpropanal and Phosphoric Acid
METHAMPHETAMINE PRODUCTION: MORE METHODS
Preparation of Methamphetamine from Chloro-ephedrin
Methamphetamine from Ephedrine
Using Phosphorus and Hydriodic Acid
Catalytic Hydrogenation
Preparation of Methamphetamine
Preparation of Desoxyephedrine (meth)
Methamphetamine from Ephedrine; Birch Reaction
Leuckart-Wallach Reaction:
Substituted N-Alkyl-Amphetamine From Substituted Phenylisopropyl-N-Alkylformamides Amines From Formamides
1-Phenyl-2-(formylamino)propane From Phenyl-2-propanone And Ammonium Formate
1-Phenyl-2-(formylalkylamino)propane
From Substituted P-2-P and N-AlkylformamidePreparation of 4-Methoxy-phenyl-2-methylaminopropane Using Methylamine Hydrochloride
Preparation of Phenyl-2-ethylaminopropane
Amphetamine From alpha-Bromophenylpropane
2-Bromo-1-phenylpropane from Allybenzene
Ritter Reaction
SUBSTITUTED BENZALDEHYDES
Benzaldehydes From Phenols; Duff Reaction
Benzaldehydes from Phenols; Elbs Persulfate Oxidation
Phenols From Benzaldehydes; Dakin Reaction
Mono-Alkylation of Hydroxybenzaldehydes
Benzaldehyde from Benzyl Chloride
Benzaldehydes From Propenylbenzenes
ALLY AND PROPENYLBENZENES FROM NATURAL SOURCES
Allybenzene, Propenylbenzene, Eugenol, Isoeugenol
Estragol, Anethol
Sassafras Root Bark Oil
Safrole, Isosafrol
2,4,5-Trimethoxyallybenzene (Beta-Asarone)
2,3,5,6-Tetramethoxyallybenzene and Apiol (3,4-methylenedioxy-2,5-dimethoxy-allybenzene) from Parsley Seeds
Dill Apiol, Isodill Apiol
Elemicin, Isoelemicin, Carpacin
Dimethoxypropenylbenzene from Asarone
Propenylbenzenes From Phenyl-1-Propanols
Propenylbenzenes From Allybenzene By Use of Potassium Hydroxide
Para-substituted Propenylbenzenes From Para-substituted Benzenes; Quelet Reaction
Preparation of Phenyl-1-Propanols Using the Grignard Reagent
Phenyl-1-Propanol by Reduction of Propiophenone
PREPARATION OF NITROALKANES FROM ALKANES
Manufacture of Nitroalkanes
Preparation of Nitroethane
Stereochemistry
Separation of d-Phenylpropanolamine
Amphetamine Syntheses: Industrial is an asset and essential reading for anyone interested in the study and synthesis of psychedelic and psychostimulant amphetamines and phenylethylamines. Considered to be the most comprehensive overview on the subject.
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