Fabrication of TiO2 Nanotubes Using Electrochemical Anodization: TiO2 Nanotubes

Abdul Muhsien Hassan, Marwa, Al-Eqaby, Haidar H.Hamdan

ISBN 10: 3659157724 / ISBN 13: 9783659157721

Published by LAP LAMBERT Academic Publishing, 2012

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Bibliographic Details

• Title: Fabrication of TiO2 Nanotubes Using Electrochemical Anodization: TiO2 Nanotubes
• Publisher: LAP LAMBERT Academic Publishing
• Publication Date: 2012
• Language: English
• ISBN 10: 3659157724
• ISBN 13: 9783659157721
• Binding: Paperback
• Condition: Like New
• Book Type: book

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Synopsis

In this work, describes the synthesis of self-organized titanium dioxide nanotube layers by an electrochemical anodization of Ti at different conditions (time, voltage, concentration of NH4F in electrolyte with glycerol, conductivity and water content) at room temperature (~25ºC) were investigated. In the current study, self-organized,vertically-oriented TiO2 nanotubes were successfully prepared by anodization method of a pure Titanium sheet (99.5%) using anodization cell is designed for first time in Iraq (Homemade) from Teflon material according to our knowledge to produce self-ordered Titanium nanotube in organic based electrolytes (glycerol based electrolyte) an electrolyte solution containing (0.5, 1, 1.5 and 2 wt.% NH4F) then added water (2 and 5Wt.% H2O) to (0.5wt.% NH4F) only with 15V. The range of anodizing time and potential were between 1-4hr. and 5-40V, where Wt.% represent weight percentage. Scanning electron microscopy (SEM), Atomic force microscopy (AFM) and (XRD) X-Ray diffraction were employed to characterize the morphology and structure of the obtained Titania templates, optical interferometer (Fizeau frings) method to tubes length measurement.

About the Author

Haidar H.Hamdan Al-Eqaby and Marwa Abdul Muhsien Hassan Al-Janabi received the B.Sc degree in physics from Al-Mustansiriyah university, Iraq in 2007 and M.Sc degree in Department of Physics from Baghdad and Al-Mustansiriyah university, Iraq in 2012 and 2010 respectively.