Neuware - This text provides details of the cross-polarization (CP) magic angle spinning (MAS) experiment as it is used to obtain rare-spin, high resolution NMR spectra. The design of CP/MAS expriments, the interpretation of spectra and relaxation measurements are covered in detail. This text explains clearly the underlying principles of NMR, as well as those involved in this particular experimental method. it can be used by either the student or the working spectroscopistneeding to learn the underlying principles of the laboratory experiments they are using.

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Bibliographic Details

Title: High Resolution NMR in the Solid State
Publisher: Oxford University Press Inc Aug 1994
Publication Date: 1994
Language: English
ISBN 10: 0195073800
ISBN 13: 9780195073805
Binding: Buch
Condition: Neu
Weight: 440 grams

About this title

Synopsis

This text was developed from a course for physical chemistry and chemical physics students using cross-polarization (CP) magic angle spinning (MAS) NMR in their laboratory assignments. The book provides students with the details of the CP/MAS experiment as it is used to obtain rare-spin, high-resolution NMR spectra. The design of the CP/MAS experiments and the interpretation of spectra and relaxation measurements require an understanding of the interplay of several fundamental physical interactions not normally encountered in solution NMR. The student can observe the way interacting spin systems behave in the solid state, and have a quantum mechanically rigorous understanding of solid-state spin phenomena. The text will have the added benefit of serving as a self-study resource for students seeking to learn the underlying principles of laboratory experiments using the technique. The history of NMR is also treated, and the instrumentation of the spectrometer and probe are discussed.

About the Author

E. O. Stejskal is at North Carolina State University.

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