Synopsis
The aim of the Polymer Reference Book is to familiarise the reader with all aspects of the techniques used in the examination of polymers, including chemical, physico-chemical and purely physical methods of examination. This book describes the types of techniques now available to the polymer chemist and technician, and discusses their capabilities, limitations and applications. All types of modern instrumentation are covered including those used in general quality control, research analysis, process monitoring and for determining the mechanical, electrical, thermal and optical characteristics. Aspects such as automated analysis and computerised control of instruments are also included. The book covers not only instrumentation for the determination of metals, non metals, functional groups, polymer structural analysis and end-groups in the main types of polymers now in use commercially, but also the analysis of minor non-polymeric components of the polymer formulation, whether they be deliberately added, such as processing additives, or whether they occur adventitiously, such as residual volatiles and monomers and water. Fingerprinting techniques for the rapid identification of polymers and methods for the examination of polymer surfaces and polymer defects are also discussed. The book gives an up-to-date and thorough exposition of the present state-of-the-art of the theory and availability of instrumentation needed to effect chemical and physical analysis of polymers. Over 1,800 references are included. The book should be of great interest to all those who are engaged in the examination of polymers in industry, university research establishments and general education. The book is intended for all staff who are concerned with instrumentation in the polymer laboratory, including laboratory designers, work planners, chemists, engineers, chemical engineers and those concerned with the implementation of specifications and process control.
About the Author
Roy Crompton was Head of the polymer analysis research department of a major international polymer producer for some 15 years. In the early fifties he was heavily engaged in the development of methods of analysis for low-pressure polyolefins produced by the Ziegler-Natta route, including work on high-density polyethylene and polypropylene. He was responsible for the development of methods of analysis of the organoaluminum catalysts used for the synthesis of these polymers. He was also responsible for the development of thin-layer chromatography for the determination of various types of additives in polymers and did pioneering work on the use of TLC to separate polymer additives and to examine the separated additives by infrared and mass spectrometry. He retired in 1988 and has since been engaged as a consultant in the field of analytical chemistry and has written extensively on this subject, with some 20 books published.
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