Title: A Revision of the Atomic Weight of Antimony the Analysis of Antimony Bromide
Publisher: Forgotten Books
Publication Date: 2018
Language: English
ISBN 10: 1332240445
ISBN 13: 9781332240449
Binding: PAP
Condition: New
Weight: 109 grams

About this title

Synopsis

Learn how antimony bromide was prepared and precisely analyzed to determine its atomic weight.

This study details careful methods, measurements, and checks that underpinned early 20th‑century chemical analysis.

In this dissertation, the author describes the apparatus, preparation steps, and analytical techniques used to study antimony bromide. It covers how samples were made, distilled, and weighed, with attention to avoiding air exposure and controlling temperature and pressure. The work combines volumetric and gravimetric approaches to cross‑check results and discusses the role of corrections and refinement in pursuing reliable values.

Step‑by‑step preparation of antimony bromide and careful control of the distillation process
Use of a nephelometric end‑point and gravimetric methods to determine silver and silver bromide ratios
Balancing precision with practicalities, including vacuum corrections and weight calibration
Discussion of multiple preparation series (B, C, D) and how consistency was assessed

Ideal for readers with an interest in the history of chemical analysis, atomic weight determination, and classic laboratory techniques.

"About this title" may belong to another edition of this title.

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