Sampling and Sample Preparation

Markus Stoeppler (editor)

ISBN 10: 3540619755 / ISBN 13: 9783540619758

Published by Springer-Verlag, 1997

About this Item

German translation. The boards show light scuffing to the corners and spine head and tail, light marking, plus a little surface lifting at the spine tail where tape has been removed. 'Received 16 Mar 1998' stamp to front end paper, plus small green clover stamp. Internally the book is in fine condition, the leaves undamaged and the pages clean. Measures 24.1 x 16.1 x 1.8cm. 202 pages.

Seller Inventory # 860

Bibliographic Details

• Title: Sampling and Sample Preparation
• Publisher: Springer-Verlag
• Publication Date: 1997
• Language: English
• ISBN 10: 3540619755
• ISBN 13: 9783540619758
• Binding: Hardcover
• Condition: Very Good
• Weight: 450 grams

About this title

Synopsis

The significant progress achieved in modern instrumental analysis has led to a continuous lowering of detection limits and improved precision. This should in principle permit the reliable and extremely precise analysis of trace compounds mainly trace elements, at levels down to the lowest natural concentrations. However, the frequently observed very high discrepancies between the analyt­ ical results of different laboratories as well as the deviations from true values are, regrettably, still common in analytical practice. Basic methodological errors at the determination step can usually be minimized or even avoided by carefully per­ formed quality control measures - e. g. by interlaboratory comparisons and the proper use of certified reference materials. The most severe and often under­ estimated error sources, however, are those connected with the whole and often extremely complex sampling process, and also to a lesser extent, with sample pre­ paration prior to analysis. Thus, for these initial steps of an analytical procedure particular experience is needed, as well as a detailed knowledge of the interrela­ tions between these steps, which always have to be applied with the utmost care. In collaboration with a number of very experienced colleagues working in dif­ book has tried to contribute to a better ferent research areas, the editor of this understanding of these particular error sources and how they can be overcome in a series of training courses held during the last decade at the "Haus der Technik", Essen, Germany.

From the Back Cover

This book describes in great detail sampling and sample preparation in routine and research. All chapters are written for practitioners by experts in the field. The book provides well-documented and illustrated procedures for sampling and sample preparation prior to trace metal analysis. A careful selection of appropriate references to pitfalls, methods and strategies furnishes the information for a proper performance of the most crucial steps of any analytical procedure.