Synopsis:
Step-by-step instructions on identifying organic compounds. The steps described include elemental analysis, solubility, infrared spectra, nuclear magnetic resonance spectra, mass spectra, classification tests, and preparation of a derivative. Most directions for experiments are described in a micro or mini scale and clean up directions are given at the end of each procedure.Emphasizes the systematic approach to identifying unknowns.-- Offers a review of spectroscopy.-- Discusses infrared, nuclear magnetic resonance, and mass spectroscopy and includes examples of spectra.-- Discusses chromatography, distillations, and the separation of mixtures.
From the Publisher:
Approaches the identification and characterization of organic compounds by integrating chemical, spectral, and other modern instrument techniques. Includes spectral and chromatographic procedures; explicit, easy instructions for operating instruments commonly found in academic organic laboratories; new, reliable wet tests; and many additional tables of useful data.
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